4-[4-(4-Chlorophenoxy)phenyl]-4-oxobut-2-enoic acid → Ethyl 4-[4-(4-chlorophenoxy)phenyl]-4-oxobut-2-enoate

HRID 2418161Notes

Reaction equation

HRID 2418161 reaction equation
[Cl:1][C:2]1[CH:21]=[CH:20][C:5]([O:6][C:7]2[CH:19]=[CH:18][C:10]([C:11]([CH:13]=[CH:14][C:15]([OH:17])=[O:16])=[O:12])=[CH:9][CH:8]=2)=[CH:4][CH:3]=1.O(C1C=CC(C(C=CC(O)=O)=O)=CC=1)[C:23]1C=CC=C[CH:24]=1>>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([O:6][C:7]2[CH:8]=[CH:9][C:10]([C:11]([CH:13]=[CH:14][C:15]([O:17][CH2:23][CH3:24])=[O:16])=[O:12])=[CH:18][CH:19]=2)=[CH:20][CH:21]=1

Participants

3

Reactant 2

HCID 543581194-[4-(4-Chlorophenoxy)phenyl]-4-oxobut-2-enoic acidHCID 54511907HCID 54511907, compound

Product 1

HCID 54084500Ethyl 4-[4-(4-chlorophenoxy)phenyl]-4-oxobut-2-enoate

Procedure

The procedure in Example 13(1) was followed, except that 6.05 g of 3-[4-(4-chlorophenoxy)benzoyl]acrylic acid were used in place of 3-(4-phenoxybenzoyl)acrylic acid, to give 5.51 g of ethyl 3-[4-(4-chlorophenoxy)benzoyl]acrylate.

Sources & evidence

ORD record
ord-506c1b84a7274fa48ec831ec4a41b1a4
Source dataset
uspto-grants-1984_09
Patent number
US04472316

Reaction notes

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