2,6-Dimethylmorpholine, cis- → HCID 54239494, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 164 g of (VI) and 159 g of 2,6-cis-dimethylmorpholine was stirred for 6 hours at 150° C. The crude product was dissolved in CHCl3, and the solution was washed with dilute aqueous NaOH and then with water, dried over Na2SO4 and concentrated. Distillation of the residue gave a yield of 147 g of (VII) of boiling point 214°-218° C./0.3 mbar.

Provenance & Evidence