Hydrochloric Acid → HCID 86739646, compound

Participants

Reaction Steps

Hydrogen chloride is introduced for 10 minutes into a solution of 5.25 g (15.05 mmol) of 2-amino-2'-[o-chloro-α-(hydroxyimino)-benzyl]-4'-nitro-acetanilide in 300 ml of methylene chloride and 100 ml of ethanol. The solution is evaporated to dryness in vacuo and the residue is dried overnight in vacuo. There is obtained 2-amino-2'-[o-chloro-α-(hydroxyimino)benzyl]-4'-nitro-acetanilide hydrochloride of melting point 140° (decomposition).

Provenance & Evidence