HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Cresol → Ethyl 2-[2-nitro-3-(o-tolyloxy)phenyl]acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Cresol | HCID 335 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Ethyl 2-(3-chloro-2-nitrophenyl)acetate | HCID 20446267 | — |
| Product | Ethyl 2-[2-nitro-3-(o-tolyloxy)phenyl]acetate | HCID 20446169 | — |
Reaction Steps
A mixture of o-cresol (4.9 g.), ethyl 2-(2-nitro-3-chlorophenyl)acetate (10.0 g.), potassium carbonate (8.5 g.) and cupric oxide (1 g.) was treated in a similar manner to the above to give the captioned compound (3.4 g.). bp 173° to 176° C./0.2 to 0.4 mmHg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04472433 |
| Source dataset | uspto-grants-1984_09 |
| ORD ID | ord-2e0d45d2d0b74b37984961749dd7cdab |
| Source note | uspto-grants-1984_09 |