HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dimethylphenol → Ethyl 2-[2-nitro-3-(3,4-dimethylphenoxy)phenyl]acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dimethylphenol | HCID 7249 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Ethyl 2-(3-chloro-2-nitrophenyl)acetate | HCID 20446267 | — |
| Product | Ethyl 2-[2-nitro-3-(3,4-dimethylphenoxy)phenyl]acetate | HCID 20446195 | — |
Reaction Steps
A mixture of ethyl 2-(2-nitro-3-chlorophenyl)acetate (10 g), 3,4-dimethylphenol (5.5 g.), anhydrous potassium carbonate (8.5 g.) and cupric oxide (1 g.) was treated in a similar manner to the above to give the captioned compound (3.65 g.). bp 190° to 196° C./0.8 mmHg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04472433 |
| Source dataset | uspto-grants-1984_09 |
| ORD ID | ord-4ded4cc36fad4f36ada47044937c98ab |
| Source note | uspto-grants-1984_09 |