HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70039995, compound → HCID 54079365, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70039995 | HCID 70039995 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 54079365 | HCID 54079365 | — |
Reaction Steps
The oily diethylphosphoryl-L-alanyl-L-proline benzylester (8.5 g, 20.6 m mole) was dissolved in methanol and palladium-carbon (2 g) was added thereto. The reductive reaction was carried out for 3 hours. The catalyst was removed by filtration and the solvent was distilled off under reduced pressure to obtain an oily diethylphosphoryl-L-alanyl-L-proline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04472381 |
| Source dataset | uspto-grants-1984_09 |
| ORD ID | ord-88b52b94162242b0b54b55188059a282 |
| Source note | uspto-grants-1984_09 |