Potassium Hydroxide → HCID 23696985, compound

HRID 2418522Notes

Reaction equation

HRID 2418522 reaction equation
[CH2:1]([P:8]([NH:17][C@H:18]([C:20]([N:22]1[CH2:36][CH2:35][CH2:34][C@H:23]1[C:24]([N:26]1[CH2:33][CH2:32][CH2:31][C@H:27]1[C:28]([OH:30])=[O:29])=[O:25])=[O:21])[CH3:19])([CH2:10][C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)=[O:9])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[OH-].[K+:38]>>[K+:38].[CH2:1]([P:8]([NH:17][C@H:18]([C:20]([N:22]1[CH2:36][CH2:35][CH2:34][C@H:23]1[C:24]([N:26]1[CH2:33][CH2:32][CH2:31][C@H:27]1[C:28]([O-:30])=[O:29])=[O:25])=[O:21])[CH3:19])([CH2:10][C:11]1[CH:12]=[CH:13][CH:14]=[CH:15][CH:16]=1)=[O:9])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 14797Potassium HydroxideHCID 13503349HCID 13503349, compound

Product 1

HCID 23696985HCID 23696985, compound

Procedure

To the oily dibenzylphosphoryl-L-alanyl-L-prolyl-L-proline, (2.72 g, 5 m mole) 0.1N potassium hydroxide (50 ml) was added, and the thus produced solution was freeze-dried to obtain an amorphous powder of the dibenzylphosphoryl-L-alanyl-L-prolyl-L-proline potassium salt (2.8 g).

Workup

  1. customthe thus produced solution was freeze-dried

Sources & evidence

ORD record
ord-070e96664eba42718539be0ea2e33f2b
Source dataset
uspto-grants-1984_09
Patent number
US04472381

Reaction notes

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