Sodium Methoxide → HCID 70497553, compound

HRID 2418680Notes

Reaction equation

HRID 2418680 reaction equation
CS[C:3]1[N:8]2[C:9]([C:12]3[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=3)=[N:10][CH:11]=[C:7]2[CH:6]=[C:5]([S:18][CH3:19])[N:4]=1.C[O-:21].[Na+]>>[CH3:19][S:18][C:5]1[CH:6]=[C:7]2[CH:11]=[N:10][CH:9]([C:12]3[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=3)[N:8]2[C:3](=[O:21])[N:4]=1

Participants

3

Reactant 2

HCID 10942334Sodium MethoxideHCID 13339916HCID 13339916, compound

Product 1

HCID 70497553HCID 70497553, compound

Procedure

Using the method of Part H, Example 1, 5,7-bis(methylthio)-3-phenylimidazo[1,5-c]pyrimidine was reacted with aqueous sodium methoxide to provide 7-methylthio-3-phenylimidazo[1,5-c]pyrimidin-5-one, m.p. 198°-199° C. Analysis: Calculated for C13H11N3OS: %C, 60.7; %H, 4.3; %N, 16.3; Found: %C, 60.7; %H, 4.1; %N, 16.7.

Sources & evidence

ORD record
ord-20154af24be645ac80312db9fffcaeb2
Source dataset
uspto-grants-1984_09
Patent number
US04473570

Reaction notes

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