Boron tribromide → HCID 131713825, compound

HRID 2418707Notes

Reaction equation

HRID 2418707 reaction equation
Cl.[NH2:2][CH2:3][C:4]1[C:13]2[C:8](=[C:9]([N:22](CC3C=CC=CC=3)[S:23]([CH3:26])(=[O:25])=[O:24])[C:10]([O:14]CC3C=CC=CC=3)=[CH:11][CH:12]=2)[CH2:7][CH2:6][CH:5]=1.B(Br)(Br)[Br:35]>C(Cl)Cl>[BrH:35].[NH2:2][CH2:3][C:4]1[C:13]2[C:8](=[C:9]([NH:22][S:23]([CH3:26])(=[O:25])=[O:24])[C:10]([OH:14])=[CH:11][CH:12]=2)[CH2:7][CH2:6][CH:5]=1

Participants

4

Reactant 2

HCID 25134Boron tribromideHCID 13340052HCID 13340052, compound

Product 1

HCID 131713825HCID 131713825, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

The dibenzyl compound of Example 32 is treated with BBr3 in CH2Cl2 to yield 1-aminomethyl-3,4-dihydro-6-hydroxy-5-methanesulfonylamino naphthalene HBr.

Sources & evidence

ORD record
ord-f8192c47eb45402589d412f9b845560a
Source dataset
uspto-grants-1984_09
Patent number
US04473586

Reaction notes

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