HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 70508417, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Trimethylsilyl cyanide | HCID 82115 | — |
| Reactant | HCID 20445304 | HCID 20445304 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | HCID 70508417 | HCID 70508417 | — |
Reaction Steps
5-methylthio-8-methoxy-1,2,3,4-tetrahydro-1-naphthalenone is reacted with trimethylsilylcyanide followed by lithium aluminum hydride, and the resulting intermediate hydroxy amino compound is dehydrated with HCl, according to the procedure of Examples 1 and 3, to yield 1-aminomethyl-5-methylthio-8-methoxy-3,4-dihydronaphthalene HCl.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04473586 |
| Source dataset | uspto-grants-1984_09 |
| ORD ID | ord-35a0c1b0977a4f7fba88aba784af920c |
| Source note | uspto-grants-1984_09 |