HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 70508328, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diboron | HCID 6328200 | — |
| Reactant | 1-(Aminomethyl)-5,6-dimethoxy-1,2,3,4-tetrahydronaphthalen-1-ol | HCID 13340002 | — |
| Reactant | HCID 20426668 | HCID 20426668 | — |
| Product | HCID 70508328 | HCID 70508328 | — |
Reaction Steps
1-aminomethyl-5,6-dimethoxy-1-hydroxy-1,2,3,4-tetrahydronaphthalene is reacted with the acid chloride of 4-chloro-2,6-dimethoxyphenoxy acetic acid. The resulting amide is reduced with diborane and dehydrated with HCl as described in Example 30 to obtain 1-[2(4-chloro-2,6-dimethoxyphenoxy)ethylaminomethyl]-5,6dimethoxy-3,4-dihydronaphthalene HCl.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04473586 |
| Source dataset | uspto-grants-1984_09 |
| ORD ID | ord-68f82722447a41aeb936aaf94da98e1c |
| Source note | uspto-grants-1984_09 |