Trityl chloride → HCID 54453593, compound

Participants

Reaction Steps

0.14 mole of triphenylchloromethane and 0.14 mole of N-hydroxy tetrapropenylsuccinimide are dissolved in 100 milliliters of dimethylformamide. 50 milliliters of triethylamine are added and the mixture is stirred overnight at room temperature. The solvent is then removed under vacuum and the reaction product is water washed until salt free and then dried. A yield of 90% of N-trityloxy tetrapropenylsuccinimide is recovered.

Provenance & Evidence