HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylenediamine → N,N'-Bis(2,2,6,6-tetramethyl-4-piperidyl)ethylenediamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylenediamine | HCID 3301 | — |
| Reactant | 2,2,6,6-Tetramethyl-4-piperidone | HCID 13220 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | N,N'-Bis(2,2,6,6-tetramethyl-4-piperidyl)ethylenediamine | HCID 3017249 | — |
Reaction Steps
162.75 g (1.05 moles) of 2,2,6,6-tetramethyl-4-piperidone dissolved in 200 cc of methanol, 30 g (0.5 moles) of ethylenediamine dissolved in 40 cc of methanol, and 0.5 g of Pt (at 10% on carbon) were introduced into a 1 liter autoclave, and the mixture hydrogenated at 80° C and 50 atm pressure for 2 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04104248 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-0b26540386b747f9bac9af6323b850b4 |
| Source note | uspto-grants-1978_08 |