5-(Chloromethyl)-1,2,3-trimethoxybenzene → HCID 12737004, compound
Reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:8]=[C:9]([O:13][CH3:14])[C:10]=1[O:11][CH3:12])[CH2:6]Cl.[C:15]1([CH:21]2[CH2:26][NH:25][CH2:24][C:23]3[S:27][CH:28]=[CH:29][C:22]2=3)[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>>[C:15]1([CH:21]2[CH2:26][N:25]([CH2:6][C:5]3[CH:4]=[C:3]([O:2][CH3:1])[C:10]([O:11][CH3:12])=[C:9]([O:13][CH3:14])[CH:8]=3)[CH2:24][C:23]3[S:27][CH:28]=[CH:29][C:22]2=3)[CH:16]=[CH:17][CH:18]=[CH:19][CH:20]=1Participants
3
Procedure
3,4,5-Trimethoxy-benzyl chloride is condensed with 4-phenyl-4,5,6,7-tetrahydro-thieno[2,3-c]pyridine (Example 3), according to the procedure of Example 8.
Sources & evidence
- ORD record
- ord-bd1cececa5294c9dbc51ac310124fb49
- Source dataset
- uspto-grants-1978_08
- Patent number
- US04104390
Reaction notes
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