Benzyl Chloride → HCID 12737009, compound

HRID 2419029Notes

Reaction equation

HRID 2419029 reaction equation
[CH2:1](Cl)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:9]1([CH:15]2[CH2:20][NH:19][CH2:18][C:17]3[CH:21]=[CH:22][S:23][C:16]2=3)[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1.C([O-])(=O)/C=C/C([O-])=O>>[CH2:1]([N:19]1[CH2:20][CH:15]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)[C:16]2[S:23][CH:22]=[CH:21][C:17]=2[CH2:18]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

4

Reactant 3

HCID 7503Benzyl ChlorideHCID 5460307FumarateHCID 12736997HCID 12736997, compound

Product 1

HCID 12737009HCID 12737009, compoundYield 34%

Procedure

Benzyl chloride is condensed with 7-phenyl-4,5,6,7-tetrahydro-thieno[3,2-c]pyridine (Example 4), according to the procedure of Example 8. Fumarate: M.p. = 200° C; yield: 34%.

Sources & evidence

ORD record
ord-43b0f7f5779948e188929231366fa1e5
Source dataset
uspto-grants-1978_08
Patent number
US04104390

Reaction notes

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