Phenethyl bromide → HCID 12737008, compound
Reaction equation
[CH2:1](Br)[CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[C:10]1([CH:16]2[CH2:21][NH:20][CH2:19][C:18]3[S:22][CH:23]=[CH:24][C:17]2=3)[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1>>[CH2:1]([N:20]1[CH2:21][CH:16]([C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[C:17]2[CH:24]=[CH:23][S:22][C:18]=2[CH2:19]1)[CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1Participants
3
Procedure
Phenethyl bromide is condensed with 4-phenyl-4,5,6,7-tetrahydro-thieno[2,3-c]pyridine (Example 3), according to the procedure of Example 8. Base: M.p. = 110° C; yield: 59%.
Sources & evidence
- ORD record
- ord-65d26b3081a344ada4d8ae6ecfffdeb2
- Source dataset
- uspto-grants-1978_08
- Patent number
- US04104390
Reaction notes
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