N-(2-{[(2-Amino-1,3-thiazol-4-yl)methyl]sulfanyl}ethyl)-N'-methylthiourea → HCID 178484987, compound

HRID 2419066Notes

Reaction equation

HRID 2419066 reaction equation
[CH3:1][NH:2][C:3]([NH:5][CH2:6][CH2:7][S:8][CH2:9][C:10]1[N:11]=[C:12]([NH2:15])[S:13][CH:14]=1)=S.[N:16]#[C:17][NH2:18].[Pb]>>[C:17]([NH:18][C:3]([NH:2][CH3:1])=[N:5][CH2:6][CH2:7][S:8][CH2:9][C:10]1[N:11]=[C:12]([NH2:15])[S:13][CH:14]=1)#[N:16]

Participants

3

Reactant 2

HCID 12923383N-(2-{[(2-Amino-1,3-thiazol-4-yl)methyl]sulfanyl}ethyl)-N'-methylthioureaHCID 22262466CH2N2Pb

Product 1

HCID 178484987HCID 178484987, compound

Procedure

Reaction of N-methyl-N'-[2-((2-amino-4-thiazolyl)-methylthio)ethyl]thiourea with lead cyanamide by the procedure of Example 91, refluxing for 24 hours, gives the title compound.

Workup

  1. temperaturerefluxing for 24 hours

Sources & evidence

ORD record
ord-da011bcd82e8418cb68cee97655c1dcb
Source dataset
uspto-grants-1978_08
Patent number
US04104382

Reaction notes

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