HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4-(2-Cyanoethyl)benzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-(2-Cyanoethyl)benzoic acid | HCID 19879196 | — |
| Product | 4-(2-Cyanoethyl)benzoyl chloride | HCID 45081714 | — |
Reaction Steps
A mixture of 17.5 parts of 4-(2-cyanoethyl) benzoic acid and 120 parts of thionyl chloride are refluxed for 15 minutes. The surplus thionyl chloride is then eliminated under reduced pressure and the 4-(2-cyanoethyl) benzoyl chloride is obtained which is liquid at atmospheric temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04105653 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-b85f3302ff164b3e8b5a66708f9a1a96 |
| Source note | uspto-grants-1978_08 |