HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 178460683, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 2,4,6-Tribromoaniline | HCID 8986 | — |
| Reactant | [2-(Chloroformyl-)2-(methyl)ethyl-]methyl phosphinic acid chloride | HCID 54003998 | — |
| Product | HCID 178460683 | HCID 178460683 | — |
Reaction Steps
330 g (1 mol) of 2,4,6-tribromoaniline was reacted as described in Example 1 with 207 g (1.02 mol) of [2-(chloroformyl-)2-(methyl)ethyl-]methyl phosphinic acid chloride (prepared as described by V. K. Khairullin et al., C.A. 69, 106816 k (1968)). After hydrolysis with 6 liters of water, the resulting [2-(2,4,6-tribromophenylcarbamoyl-) 2-(methyl)ethyl-]methyl phosphinic acid was filtered off and dried at 80° C under vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04105689 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-fec1a8bdd3a7421f978ddd31854bd6cd |
| Source note | uspto-grants-1978_08 |