1H-Imidazole, 1-[2-(2,4-dichlorophenyl)hexyl]- → HCID 70588101, compound

HRID 2419327Notes

Reaction equation

HRID 2419327 reaction equation
[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[CH:9]([CH2:16][CH2:17][CH2:18][CH3:19])[CH2:10][N:11]1[CH:15]=[CH:14][N:13]=[CH:12]1>CCOCC>[ClH:1].[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[CH:9]([CH2:16][CH2:17][CH2:18][CH3:19])[CH2:10][N:11]1[CH:15]=[CH:14][N:13]=[CH:12]1

Participants

3

Reactant 1

HCID 30068521H-Imidazole, 1-[2-(2,4-dichlorophenyl)hexyl]-

Product 1

HCID 70588101HCID 70588101, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

In 30.0 g (0.101 mole) of 1-[β-(2,4-dichlorophenyl)hexyl]imidazole dissolved in 200 ml of ether is bubbled dry hydrogen chloride gas until the mixture is acidic to litmus. A colorless solid forms which is separated by filtration to give 24.5 g. of the hydrochloride salt which is identified by nmr.

Workup

  1. customis bubbled dry hydrogen chloride gas until the mixture
  2. customA colorless solid forms which is separated by filtration
  3. customto give 24.5 g

Sources & evidence

ORD record
ord-bcc280f5ded64ec88bb48482a36437e9
Source dataset
uspto-grants-1978_08
Patent number
US04105762

Reaction notes

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