HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → HCID 20306119, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | 1H-Imidazole, 1-[2-(2,4-dichlorophenyl)hexyl]- | HCID 3006852 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Product | HCID 20306119 | HCID 20306119 | — |
Reaction Steps
To a solution of 40 ml of nitric acid and 10 ml of sulfuric acid, 14.8g (0.0498 mole) of 1-[β-(2,4-dichlorophenyl)hexyl]imidazole in 30 ml of sulfuric acid is added at less than 5°. The reaction is stirred for 1/2 hour and then it is poured into iced water. The oily solid which separates is isolated by decanting off the dilute acid solution. The residue is washed and then treated with ammonium hydroxide solution.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04105762 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-7a0a59268e524036997350d0c2793cf0 |
| Source note | uspto-grants-1978_08 |