Methanol → HCID 54482457, compound
Reaction equation
[CH3:1][N:2]1[CH:6]=[C:5]([CH:7]=[CH:8][C:9](Cl)=[O:10])[C:4]([N+:12]([O-:14])=[O:13])=[N:3]1.[CH3:15][OH:16]>>[CH3:1][N:2]1[CH:6]=[C:5]([CH:7]=[CH:8][C:9]([O:16][CH3:15])=[O:10])[C:4]([N+:12]([O-:14])=[O:13])=[N:3]1Participants
3
Procedure
The same product is obtained when 0.22 g. of the 3-(1-methyl-3-nitro-4-pyrazolyl)-acrylic acid chloride described in Example 2 is allowed to react in 1.8 ml. methanol for 30 minutes at ambient temperature and the resultant crystals filtered off with suction.
Workup
- customThe same product is obtained when 0.22 g
- customto react in 1.8 ml
- filtrationthe resultant crystals filtered off with suction
Sources & evidence
- ORD record
- ord-fc720393c5b74998a12a24101dfc1f89
- Source dataset
- uspto-grants-1978_08
- Patent number
- US04105772
Reaction notes
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