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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2419479Generated: November 1, 2026

Diethyl Ether → Sulfuric Acid

https://huagongshe.com/reaction/2419479

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiethyl EtherHCID 3283—
ReactantHCID 86735919HCID 86735919—
SolventIsopropanol heptaneHCID 21225753—
ProductSulfuric AcidHCID 1118—
ProductTriphenylphosphineHCID 11776—

Reaction Steps

18.6 g (0.05 mole) of this ether of 20 carbon atoms are reacted, in accordance with German Pat. No. 1,068,709, with 0.05 mole of triphenylphosphine and 0.05 mole of H2SO4 in isopropanol/heptane to give the corresponding 3,7,11,15-tetramethyl-hexadeca-2,4,6,8,10-pentaen-1-yl-triphenylphosphonium bisulfate.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04105855
Source datasetuspto-grants-1978_08
ORD IDord-ab5a148e24f14a96ab05ed60f1ce434a
Source noteuspto-grants-1978_08