HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2419503Generated: October 31, 2026
2-Methoxy-5-nitroaniline → HCID 20313363, compound
https://huagongshe.com/reaction/2419503
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-Methoxy-5-nitroaniline | HCID 7447 | — |
| Reactant | HCID 53934448 | HCID 53934448 | — |
| Product | HCID 20313363 | HCID 20313363 | 85% |
Reaction Steps
A mixture of 21.8 g of ethyl (2-ethylthio-2-methylpropionyl)acetate obtained in Step 1 of Synthesis Example 1 and 16.8 g of 2-methoxy-5-nitroaniline was stirred in an oil bath at 150° C for four hours under a reduced pressure of 50 to 100 mmHg. The reaction mixture was recrystallized from acetonitrile to obtain 29 g (yield 85%) of Coupler (7) having a melting point of 138° to 140° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04106942 |
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| Source dataset | uspto-grants-1978_08 |
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| ORD ID | ord-feb974b97f324cccb53c017e609db5e5 |
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| Source note | uspto-grants-1978_08 |
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