o-(Octadecyloxy)aniline → HCID 54083122, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 21.8 g of ethyl (2-ethylthio-2-methylpropionyl)acetate obtained in Step 1 of Synthesis Example 1 and 36.1 g of 2-octadecyloxyaniline was stirred in an oil bath at 150° C for 4 hours under a reduced pressure of 50 to 100 mmHg. The reaction mixture was recrystallized from ethanol to obtain 45.3 g (yield 85%) of Coupler (10) having a melting point of 60° to 62° C.

Provenance & Evidence