HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54558425, compound → HCID 53719004, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54558425 | HCID 54558425 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 53719004 | HCID 53719004 | — |
Reaction Steps
45 g of (0.134 mol) of 2,6-dinitro-4-carbomethoxybenzene-phosphonic acid dimethylester are dissolved in 550 ml of methanol and hydrogenated at 35° C and 60 excess atmospheres after the addition of 10 g of Raney nickel. The catalyst is filtered off after 4 hours and the solvent is then evaporated off and the residue is freed from any remaining solvent in a high vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04107152 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-0e136b07d2b24eba97ba4f8a9d652eb7 |
| Source note | uspto-grants-1978_08 |