HCID 53824869, compound → HCID 54424697, compound

HRID 2419522Notes

Reaction equation

HRID 2419522 reaction equation
[CH2:1]([O:3][P:4]([C:9]1[C:14]([N+:15]([O-])=O)=[CH:13][C:12]([C:18]([O:20][CH3:21])=[O:19])=[CH:11][C:10]=1[N+:22]([O-])=O)(=[O:8])[O:5][CH2:6][CH3:7])[CH3:2]>[Ni].C(O)C>[CH2:6]([O:5][P:4]([C:9]1[C:14]([NH2:15])=[CH:13][C:12]([C:18]([O:20][CH3:21])=[O:19])=[CH:11][C:10]=1[NH2:22])(=[O:8])[O:3][CH2:1][CH3:2])[CH3:7]

Participants

4

Reactant 1

HCID 53824869HCID 53824869, compound

Product 1

HCID 54424697HCID 54424697, compound

Reagents, catalysts & solvents 2

HCID 935NickelCatalystHCID 702EthanolSolvent

Procedure

80 g (0.221 mol) of 2,6-dinitro-4-carbomethoxy-benzene-phosphonic acid diethylester, 1000 ml of ethanol and 15 g of Raney nickel.

Sources & evidence

ORD record
ord-68b5ecead1894b4b8bd43b0cda868629
Source dataset
uspto-grants-1978_08
Patent number
US04107152

Reaction notes

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