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HRID2419524

反应详情

EQUATION

反应方程式

HRID 2419524 的结构方程式

REACTANTS

反应物

2
结构：C=CCBr
HCID7841

Allyl bromide

C3H5Br

结构：CCOC(=O)CC(C)C1C(=O)NC(=O)NC1=O
HCID13023200

未命名化合物

PRODUCTS

生成物

1
结构：C=CCC1(C(C)CC(=O)OCC)C(=O)NC(=O)NC1=O
HCID13023201

未命名化合物

PROCEDURE

实验过程

5-(β-Carboethoxy-α-methyl-ethyl)-barbituric acid was treated with allyl bromide at 50° C. to afford 5-allyl-5-(β-carboethoxy-α-methyl-ethyl)-barbituric acid, m.p. 114°. Alkaline saponification of this compound afforded 5-allyl-5-(β-carboxy-α-methyl-ethyl)-barbituric acid, which was recrystallized from water, m.p. 200°.