Potassium Permanganate → HCID 2819920, compound

HRID 2419547Notes

Reaction equation

HRID 2419547 reaction equation
[S:1]([N:11]=[S:12]1[CH2:17][CH2:16][CH2:15][S:14](=[O:19])(=[O:18])[CH2:13]1)([C:4]1[CH:10]=[CH:9][C:7]([CH3:8])=[CH:6][CH:5]=1)(=[O:3])=[O:2].[Mn]([O-])(=O)(=O)=[O:21].[K+]>C(OC(=O)C)(=O)C>[S:1]([N:11]=[S:12]1(=[O:21])[CH2:17][CH2:16][CH2:15][S:14](=[O:18])(=[O:19])[CH2:13]1)([C:4]1[CH:5]=[CH:6][C:7]([CH3:8])=[CH:9][CH:10]=1)(=[O:3])=[O:2]

Participants

4

Reactant 2

HCID 516875Potassium PermanganateHCID 73676074HCID 73676074, compound

Product 1

HCID 2819920HCID 2819920, compound

Reagents, catalysts & solvents 1

HCID 7918Acetic AnhydrideSolvent

Procedure

A method as defined in claim 59 which includes the additional step of reacting said 1-tosylimino-1,3-dithiane-3,3-dioxide with potassium permanganate in acetic acid-acetic anhydride solution at about 20° to 30° C to yield the corresponding 1-tosylimino-1,3-dithiane-1,3,3-trioxide.

Workup

  1. customat about 20° to 30° C

Sources & evidence

ORD record
ord-3e61454047014c35a8e40b836a453ea9
Source dataset
uspto-grants-1978_08
Patent number
US04107176

Reaction notes

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