Sulfuric Acid → HCID 12374170, compound

HRID 2419548Notes

Reaction equation

HRID 2419548 reaction equation
S([N:11]=[S:12]1(=[O:20])[CH2:17][CH2:16][CH2:15][S:14](=[O:19])(=[O:18])[CH2:13]1)(C1C=CC(C)=CC=1)(=O)=O.S(=O)(=O)(O)O>>[NH:11]=[S:12]1(=[O:20])[CH2:17][CH2:16][CH2:15][S:14](=[O:19])(=[O:18])[CH2:13]1

Participants

3

Reactant 2

HCID 1118Sulfuric AcidHCID 2819920HCID 2819920, compound

Product 1

HCID 12374170HCID 12374170, compound

Procedure

The method of claim 61 which includes the additional step of reacting said 1-tosylimino-1,3-dithiane-1,3,3-trioxide with concentrated sulfuric acid at 25° to 90° C to yield the corresponding 1-imino-1,3-dithiane-1,3,3-trioxide.

Workup

  1. customat 25° to 90° C

Sources & evidence

ORD record
ord-97cab6f3c016431f80ce364ffbf97142
Source dataset
uspto-grants-1978_08
Patent number
US04107176

Reaction notes

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