HCID 20313651, compound → HCID 86735923, compound

HRID 2419593Notes

Reaction equation

HRID 2419593 reaction equation
[OH2:1].O.O.[ClH:4].Cl.Cl.[OH:7][C:8]1[CH:9]=[C:10]2[C:15](=[CH:16][C:17]=1O)[CH:14]([CH2:19][CH2:20][CH:21]([CH2:36][CH2:37][CH2:38][CH2:39][CH:40]1[C:49]3[C:44](=[CH:45][C:46]([OH:51])=[C:47]([OH:50])[CH:48]=3)[CH2:43][CH2:42][NH:41]1)[CH2:22][CH2:23][CH:24]1[C:33]3[C:28](=[CH:29][C:30]([OH:35])=[C:31](O)[CH:32]=3)[CH2:27][CH2:26][NH:25]1)[NH:13][CH2:12][CH2:11]2>C(O)(=O)C>[OH2:7].[OH2:1].[OH2:7].[ClH:4].[ClH:4].[ClH:4].[C:47]([OH:50])(=[O:1])[CH3:48].[C:47]([OH:50])(=[O:1])[CH3:48].[C:47]([OH:50])(=[O:1])[CH3:48].[OH:35][C:30]1[CH:29]=[C:28]2[C:33](=[CH:32][CH:31]=1)[CH:24]([CH2:23][CH2:22][CH:21]([CH2:36][CH2:37][CH2:38][CH2:39][CH:40]1[C:49]3[C:44](=[CH:45][C:46]([OH:51])=[CH:47][CH:48]=3)[CH2:43][CH2:42][NH:41]1)[CH2:20][CH2:19][CH:14]1[C:15]3[C:10](=[CH:9][C:8]([OH:7])=[CH:17][CH:16]=3)[CH2:11][CH2:12][NH:13]1)[NH:25][CH2:26][CH2:27]2

Participants

3

Reactant 1

HCID 20313651HCID 20313651, compound

Product 1

HCID 86735923HCID 86735923, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

Similarly, when 800 mg. of (10.6) is suspended in 20 ml. glacial acetic acid containing 2 g. of acetyl chloride, and dry hydrogen chloride is bubbled through the mixture, on workup

Workup

  1. customof acetyl chloride, and dry hydrogen chloride is bubbled through the mixture, on workup

Sources & evidence

ORD record
ord-2a783f12eeb34d62bf67b957d37ef464
Source dataset
uspto-grants-1978_08
Patent number
US04107165

Reaction notes

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