HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Diisopropylamino-2-phenyl-butyronitrile → alpha,alpha-Bis[2-(diisopropylamino)ethyl]-alpha-(2-pyridyl)acetonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Diisopropylamino-2-phenyl-butyronitrile | HCID 12612210 | — |
| Reactant | 4-Diisopropylamino 2-(2-pyridyl)butyronitrile | HCID 13319674 | — |
| Product | alpha,alpha-Bis[2-(diisopropylamino)ethyl]-alpha-(2-pyridyl)acetonitrile | HCID 21320525 | — |
Reaction Steps
Substitution of an equivalent quantity of the preceding acetonitrile for α-[2-(diisopropylamino)ethyl]-α-phenylacetonitrile called for in Example 2, Method B and substantial repetition of the procedure detailed in that example, affords α,α-bis[2-(diisopropylamino)ethyl]-α-(2-pyridyl)acetonitrile, as an oil boiling at about 155°-160° C. at 0.3 mm. pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04107205 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-9deea0d92c104e0da26a9d4ff47f464d |
| Source note | uspto-grants-1978_08 |