HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1-Dimethoxyhex-3-yn-2-one → HCID 57417966, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1-Dimethoxyhex-3-yn-2-one | HCID 20314017 | — |
| Solvent | Quinoline | HCID 7047 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 57417966 | HCID 57417966 | — |
Reaction Steps
Six grams of the 1,1-dimethoxy-3-hexyne-2-one (of Example I) is stirred under hydrogen gas at one atmosphere in 40 ml hexane containing 0.6 g Lindlar catalyst (palladium-on-calcium carbonate poisoned with lead acetate) and 4.0 g quinoline. The reaction is terminated when 1% of the starting material (1,1-dimethoxy-3-hexyne-2-one) remains after about 11/2 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04107217 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-2469045d4cf74f5badde306177b6b4ff |
| Source note | uspto-grants-1978_08 |