HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 5-(Methylthio)-imidazo[1,2-d]-as-triazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | Imidazo[1,2-d]-as-triazine-5(6H)-thione | HCID 12493308 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 5-(Methylthio)-imidazo[1,2-d]-as-triazine | HCID 12493310 | — |
Reaction Steps
A 66.7 gm. portion of imidazo[1,2-d]-as-triazine-5(6H)-thione is added to 250 ml. of ethanol. A solution of 10.1 gm. of sodium reacted in 250 ml. of ethanol is added with swirling. A 27.7 ml. portion of methyl iodide is added slowly with swirling. The mixture is stored in a chillroom overnight, filtered and dried giving 56.5 gm. of the desired final product, m.p. 147°-149° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04107309 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-ede1b65fcce7417db802e0a7b4ea8876 |
| Source note | uspto-grants-1978_08 |