HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 4,5-Dimethyl-2-n-propyl-2-imidazoline-4,5-diol hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Butanimidamide hydrochloride | HCID 12828983 | — |
| Product | 4,5-Dimethyl-2-n-propyl-2-imidazoline-4,5-diol hydrochloride | HCID 12493279 | — |
Reaction Steps
A 112.7 gm. portion of butyramidine hydrochloride is dissolved in 200 ml. of water. A 107 gm. portion of freshly distilled diacetyl is added and the mixture is stirred. The pH is adjusted to 6.5-7.0 with 2N NaOH and the solution is chilled. The desired product is collected as a solid, m.p. 104°-107° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04107308 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-90164dd747004374b9ce9312c0afad0f |
| Source note | uspto-grants-1978_08 |