Toluene → HCID 12493313, compound

HRID 2419669Notes

Reaction equation

HRID 2419669 reaction equation
CS[C:3]1[N:8]2[CH:9]=[N:10][CH:11]=[C:7]2[CH:6]=[N:5][N:4]=1.C[NH:13][CH2:14][CH2:15][NH:16][CH3:17].[C:18]1(C)C=CC=CC=1>>[CH3:18][N:16]([CH3:17])[CH2:15][CH2:14][NH:13][C:3]1[N:8]2[CH:9]=[N:10][CH:11]=[C:7]2[CH:6]=[N:5][N:4]=1

Participants

4

Reactant 3

HCID 1140TolueneHCID 8070N,N'-DimethylethylenediamineHCID 12493309HCID 12493309, compound

Product 1

HCID 12493313HCID 12493313, compound

Procedure

A 5.0 gm. portion of 4-(methylthio)-imidazo[1,5-d]-as-triazine in a mixture of 30 ml. of unsymmetrical dimethylethylenediamine and 20 ml. of toluene is reacted as described in Example 40 giving the desired product as light yellow crystals, m.p. 172°-177° C.

Sources & evidence

ORD record
ord-4c2a5421058c443680a8902e79f52ae9
Source dataset
uspto-grants-1978_08
Patent number
US04107308

Reaction notes

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