HCID 12493301, compound → HCID 13548779, compound

HRID 2419682Notes

Reaction equation

HRID 2419682 reaction equation
[CH3:1]C1N=CN2C=1C=NNC2=S.[CH3:12][C:13]1[N:14]=[C:15]([CH2:23][CH2:24][CH3:25])[N:16]2[C:21]=1[CH:20]=[N:19][NH:18][C:17]2=[S:22]>C1CCCCC1>[CH3:12][C:13]1[N:14]=[C:15]([CH2:23][CH2:24][CH3:25])[N:16]2[C:21]=1[CH:20]=[N:19][N:18]=[C:17]2[S:22][CH3:1]

Participants

4

Reactant 2

HCID 12493301HCID 12493301, compoundHCID 13548750HCID 13548750, compound

Product 1

HCID 13548779HCID 13548779, compound

Reagents, catalysts & solvents 1

HCID 8078CyclohexaneSolvent

Procedure

Repeating the procedure of Example 59 in every detail except that in lieu of 8-methylimidazo[1,5-d]-as-triazine-4(3H)-thione, 8-methyl-6-propylimidazo[1,5-d]-as-triazine-4(3H)-thione is employed, there is obtained the desired above-noted product having a melting point equal to 74°-78° C (cyclohexane).

Workup

  1. customthere is obtained the desired above-noted product
  2. customequal to 74°-78° C

Sources & evidence

ORD record
ord-e42c699143a34f1b9916f3f290c71ad4
Source dataset
uspto-grants-1978_08
Patent number
US04107308

Reaction notes

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