Succinic Acid → HCID 178512101, compound

HRID 2419782Notes

Reaction equation

HRID 2419782 reaction equation
[CH2:1]([NH:8][C:9]([NH:11][N:12]=[CH:13][C:14]1[C:19]([Cl:20])=[CH:18][CH:17]=[CH:16][C:15]=1[Cl:21])=[NH:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:22]([OH:29])(=[O:28])[CH2:23][CH2:24][C:25]([OH:27])=[O:26]>>[C:22]([OH:29])(=[O:28])[CH2:23][CH2:24][C:25]([OH:27])=[O:26].[CH2:1]([NH:8][C:9]([NH:11][N:12]=[CH:13][C:14]1[C:15]([Cl:21])=[CH:16][CH:17]=[CH:18][C:19]=1[Cl:20])=[NH:10])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1.[CH2:1]([NH:8][C:9]([NH:11][N:12]=[CH:13][C:14]1[C:15]([Cl:21])=[CH:16][CH:17]=[CH:18][C:19]=1[Cl:20])=[NH:10])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 1110Succinic AcidHCID 178512100HCID 178512100, compound

Product 1

HCID 178512101HCID 178512101, compound

Procedure

A solution of 2.00 g. of 1-benzyl-3-(2,6-dichlorobenzylideneamino)guanidine and 0.370 g. of succinic acid in 50 ml. of methanol is evaporated under reduced pressure, giving the desired product as a light yellow solid, m.p. 70°-80° c.

Workup

  1. customof methanol is evaporated under reduced pressure

Sources & evidence

ORD record
ord-44153f6145d94669920dbee0f03e5d12
Source dataset
uspto-grants-1978_08
Patent number
US04107326

Reaction notes

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