HRID2419782

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID1110

Butanedioic acid

C4H6O4

HCID178512100

未命名化合物

PRODUCTS

生成物

结构：N=C(NCc1ccccc1)NN=Cc1c(Cl)cccc1Cl.N=C(NCc1ccccc1)NN=Cc1c(Cl)cccc1Cl.O=C(O)CCC(=O)O

HCID178512101

未命名化合物

PROCEDURE

实验过程

A solution of 2.00 g. of 1-benzyl-3-(2,6-dichlorobenzylideneamino)guanidine and 0.370 g. of succinic acid in 50 ml. of methanol is evaporated under reduced pressure, giving the desired product as a light yellow solid, m.p. 70°-80° c.

WORKUP

后处理

customof methanol is evaporated under reduced pressure

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-44153f6145d94669920dbee0f03e5d12
来源数据集: uspto-grants-1978_08
DOI: 10.6084/m9.figshare.5104873.v1
专利: US04107326
来源说明: uspto-grants-1978_08

反应 SMILES

[CH2:1]([NH:8][C:9]([NH:11][N:12]=[CH:13][C:14]1[C:19]([Cl:20])=[CH:18][CH:17]=[CH:16][C:15]=1[Cl:21])=[NH:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:22]([OH:29])(=[O:28])[CH2:23][CH2:24][C:25]([OH:27])=[O:26]>>[C:22]([OH:29])(=[O:28])[CH2:23][CH2:24][C:25]([OH:27])=[O:26].[CH2:1]([NH:8][C:9]([NH:11][N:12]=[CH:13][C:14]1[C:15]([Cl:21])=[CH:16][CH:17]=[CH:18][C:19]=1[Cl:20])=[NH:10])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1.[CH2:1]([NH:8][C:9]([NH:11][N:12]=[CH:13][C:14]1[C:15]([Cl:21])=[CH:16][CH:17]=[CH:18][C:19]=1[Cl:20])=[NH:10])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1