Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Diphenyl Ether | HCID 7583 | — |
| Reactant | HCID 86735935 | HCID 86735935 | — |
| Product | HCID 178469186 | HCID 178469186 | 61.3% |
Reaction Steps
A suspension of 5 g of the product of Step A and 10 g of phenyl oxide was heated to 240° C and was then cooled to room temperature. The phenyl oxide was evaporated and the resulting crystals were added to 20 ml of isopropyl ether. The mixture was filtered to obtain 2.9 g of ethyl 4-hydroxy-2-methyl-8-trifluoromethyl-quinoline-3-carboxylate melting at 165° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04107310 |
|---|
| Source dataset | uspto-grants-1978_08 |
|---|
| ORD ID | ord-9c649efab57544db86768ecc07f506c2 |
|---|
| Source note | uspto-grants-1978_08 |
|---|
