Phosphorus pentachloride → HCID 20314308, compound

HRID 2419822Notes

Reaction equation

HRID 2419822 reaction equation
[F:1][C:2]([F:17])([F:16])[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[NH:9][C:10](=O)[CH2:11][CH2:12][CH2:13][CH3:14].P(Cl)(Cl)(Cl)(Cl)[Cl:19]>>[F:1][C:2]([F:17])([F:16])[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[N:9]=[C:10]([Cl:19])[CH2:11][CH2:12][CH2:13][CH3:14]

Participants

3

Reactant 2

HCID 24819Phosphorus pentachlorideHCID 2274751N-[2-(trifluoromethyl)phenyl]pentanamide

Product 1

HCID 20314308HCID 20314308, compoundYield 102.5%

Procedure

Using the procedure of Step B of Example 6, 20 g of the product of Step A and 19 g of phosphorus pentachloride were reacted to form 22.05 g of N-(2-trifluoromethylphenyl)-pentanimidoyl chloride as an oil which was used as is for the next step.

Workup

  1. customwere reacted

Sources & evidence

ORD record
ord-1f62e94c05a0462fb0564d77287caf3a
Source dataset
uspto-grants-1978_08
Patent number
US04107310

Reaction notes

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