関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 2-Ethylhexylamine | HCID 7719 | — |
| 反応物 | Ethyl cyanoacetate | HCID 7764 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 2-cyano-N-(2-ethylhexyl)acetamide | HCID 4590704 | — |
反応手順
To ethylcyanoacetate (141 g., 1.25 mole) is slowly added 2-ethylhexylamine (129 g., 1.0 mole) over a period of 0.5 hours. The solution is then gradually heated to 154° C. and the ethanol formed is collected over a period of 1.75 hours. The solution is then stripped of all volatiles boiling at or below 88° C./3.0 mm to give N-(2-ethylhexyl)cyanoacetamide, 201.5 g.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04108630 |
|---|
| 出典データセット | uspto-grants-1978_08 |
|---|
| ORD ID | ord-c74f7ebe3ab44dbe9f196bfa2e92df9b |
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| 出典メモ | uspto-grants-1978_08 |
|---|
