Hexachlorocyclotriphosphazene → p-Fluorophenoxypentachlorocyclotriphosphazene

Participants

Reaction Conditions

Reaction Steps

60 parts of hexachlorocyclotriphosphazene were charged into a reactor together with 500 parts of tetrahydrofuran, and the mixture cooled at -78° C. The previously prepared sodium p-fluorophenoxide solution was added dropwise and reacted as in Example 1. The resultant product was worked up as in Example 1 to yield p-fluorophenoxypentachlorocyclotriphosphazene (b.p. 107° C at 0.02 Torr).

Provenance & Evidence