2-methyl-2-(methylthio)propanal O-[(dibutylaminosulfenyl)(methyl)carbamoyl]-oxime → 2-methyl-2-(methylthio)propionaldehyde O-[N-methyl-N-(dimethylaminosulfenyl)carbamoyl]oxime
Reaction equation
[CH2:1]([N:5]([CH2:19]CCC)[S:6][N:7]([CH3:18])[C:8]([O:10][N:11]=[CH:12][C:13]([CH3:17])([S:15][CH3:16])[CH3:14])=[O:9])CCC.CN(C)SCl>>[CH3:19][N:5]([CH3:1])[S:6][N:7]([CH3:18])[C:8]([O:10][N:11]=[CH:12][C:13]([CH3:14])([S:15][CH3:16])[CH3:17])=[O:9]Participants
3
Procedure
2-Methyl-2-(methylthio)propanal O-[(dimethylaminosulfenyl)-(methyl)carbamoyl]oxime is prepared in the same manner as the compound of Example III except that dimethylaminosulfenyl chloride is used instead of dibutylaminosulfenyl chloride.
Sources & evidence
- ORD record
- ord-88b3f5afdf274a618febd7295b7f061f
- Source dataset
- uspto-grants-1978_08
- Patent number
- US04108991
Reaction notes
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