HCID 20313068, compound → HCID 20313101, compound

HRID 2420126Notes

Reaction equation

HRID 2420126 reaction equation
[CH2:1](OC(C1SCCSC=1CCC)=O)[CH3:2].[CH2:15]([O:17][C:18]([C:20]1[S:25](=[O:27])(=[O:26])[CH2:24][CH2:23][S:22](=[O:29])(=[O:28])[C:21]=1[CH2:30][CH2:31][CH3:32])=[O:19])[CH3:16]>>[CH2:15]([O:17][C:18]([C:20]1[S:25](=[O:26])(=[O:27])[CH2:24][CH2:23][S:22](=[O:28])(=[O:29])[C:21]=1[CH2:30][CH2:31][CH3:32])=[O:19])[CH2:16][CH2:1][CH3:2]

Participants

3

Reactant 2

HCID 20313068HCID 20313068, compoundHCID 20313106HCID 20313106, compound

Product 1

HCID 20313101HCID 20313101, compound

Procedure

By following substantially the procedure of Example 1, Step C, 3-ethoxycarbonyl-2-n-propyl-5,6-dihydro-1,4-dithiin (9.0 g.) yields 8.15 g. of 3-ethoxycarbonyl-2-n-propyl-5,6-dihydro-1,4-dithiin-1,1,4,4-tetroxide 73.5°-74.5° C.

Workup

  1. customyields 8.15 g

Sources & evidence

ORD record
ord-b253e873b3ec4b62b1cd780f97a0dcbf
Source dataset
uspto-grants-1978_08
Patent number
US04109006

Reaction notes

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