HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → HCID 86735963, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | HCID 673195 | HCID 673195 | — |
| Product | HCID 86735963 | HCID 86735963 | — |
Reaction Steps
A mixture of 2.9 g. of 2-methyl-5,7-dibromo-benzoxazole and 2.5 ml. of dimethyl-sulfate were heated at 150° C. for 5 minutes. By cooling, a solid cake was obtained. It was then ground in a mortar by washing repeatedly with ethyl ether. The product was employed without further purification for the dye synthesis.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04110116 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-81ff2340516640d7ba67a78a2e91f0ab |
| Source note | uspto-grants-1978_08 |