Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Diethyl Sulfate | HCID 6163 | — |
| Reactant | HCID 20311089 | HCID 20311089 | — |
| Product | HCID 86735965 | HCID 86735965 | — |
Reaction Steps
A mixture of 2.0 g of 2-methyl-5,7-dichloro-benzoxazole and 2.5 ml of diethyl-sulphate was heated at 150° C for 40 minutes. By cooling, a solid cake was obtained. It was then ground in a mortar by washing repeatedly with ethyl ether. The product was employed without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04110116 |
|---|
| Source dataset | uspto-grants-1978_08 |
|---|
| ORD ID | ord-f7646c0ec9064e319aca84942e59013c |
|---|
| Source note | uspto-grants-1978_08 |
|---|
