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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2420246Generated: October 25, 2026

Phosphoric Acid → 3-Azidomethyl-2-thienylacetic Acid

https://huagongshe.com/reaction/2420246

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPhosphoric AcidHCID 1004—
ReactantSulfuric AcidHCID 1118—
ReactantEthyl 3-azidomethyl-2-thienylacetateHCID 20311364—
Product3-Azidomethyl-2-thienylacetic AcidHCID 20311369—

Reaction Steps

Hydrolysis of ethyl 3-azidomethyl-2-thienylacetate by the above procedure or by employing an equal volume of 6M sulfuric acid or 8M phosphoric acid in place of the 3M hydrochloric acid also affords the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04110342
Source datasetuspto-grants-1978_08
ORD IDord-e142cf79ebb14fdebbfdaefbcbf217a0
Source noteuspto-grants-1978_08