Dimethylamine → HCID 13329795, compound

HRID 2420276Notes

Reaction equation

HRID 2420276 reaction equation
[CH2:1]=[CH:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11].[NH:12](C)[CH3:13]>C1(C)C=CC=CC=1>[CH3:1][CH:2]([CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11])[CH2:13][NH2:12]

Participants

4

Reactant 2

HCID 674DimethylamineHCID 131901-Undecene

Product 1

HCID 13329795HCID 13329795, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

20g of 1-undecene and 10g of (CH3)2NH are reacted in accordance with the method of example 3 with Zr (Me2N4) (1g) in 50ml of toluene. After 20 hours at 200° C., (N-methyl, N-2 methylundecylamine) is obtained, and is separated by chromatography on an Al2O3 column.

Sources & evidence

ORD record
ord-06e979e701dc4c6390c6578423a684ec
Source dataset
uspto-grants-1978_08
Patent number
US04110377

Reaction notes

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