Sodium Hydroxide → HCID 21314321, compound

HRID 2420373Notes

Reaction equation

HRID 2420373 reaction equation
C([O:3][C:4](=[O:16])[C:5]([NH:7][C:8]1[C:13]([C:14]#[N:15])=[CH:12][CH:11]=[CH:10][N:9]=1)=[O:6])C.[OH-].[Na+]>O>[C:14]([C:13]1[C:8]([NH:7][C:5](=[O:6])[C:4]([OH:16])=[O:3])=[N:9][CH:10]=[CH:11][CH:12]=1)#[N:15]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 12264879Acetic acid, [(3-cyano-2-pyridinyl)amino]oxo-, ethyl ester

Product 1

HCID 21314321HCID 21314321, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

(3-Cyano-2-pyridyl)oxamic acid ethyl ester (0.005 mole) is stirred in 50 ml. water and 5.0 ml. of N NaOH is slowly added. After one half hour the solution is filtered and the filtrate is acidified to pH 2 with N HCl, giving the title compound.

Workup

  1. filtrationAfter one half hour the solution is filtered

Sources & evidence

ORD record
ord-57c45b05197b4a66bcb59b1c205396b5
Source dataset
uspto-grants-1978_08
Patent number
US04110458

Reaction notes

Loading…