Bromotriphenylmethane → 3-Triphenylmethoxy-cis-oct-5-en-1-yne

Participants

Reaction Steps

Treatment of 22 g. of cis-oct-5-en-1-yne-3-ol, prepared according to the procedure of J. Fried, C. H. Lin, J. C. Sih, P. Dalven, G. F. Cooper, J. Amer. Chem. Soc., 94, 4342 (1972), with 58 g. of triphenylmethyl bromide in 100 ml. of pyridine and purification of Florisil®, all as described in Example 728 gives the title compound.

Provenance & Evidence